2-Methylbutan-2-yl prop-2-enoate → HCID 14134445, compound

HRID 986731Notes

Reaction equation

HRID 986731 reaction equation
C(OC(C)(C)CC)(=O)C=C.C[O:12][P:13]([CH:25]([NH:27]C(OCC1C=CC=CC=1)=O)[CH3:26])([CH2:15][CH:16]([C:21]([O:23]C)=[O:22])[CH2:17][CH:18]([CH3:20])[CH3:19])=[O:14]>>[NH2:27][CH:25]([P:13]([CH2:15][CH:16]([C:21]([OH:23])=[O:22])[CH2:17][CH:18]([CH3:19])[CH3:20])(=[O:12])[OH:14])[CH3:26]

Participants

3

Reactant 2

HCID 132250292-Methylbutan-2-yl prop-2-enoateHCID 67908641HCID 67908641, compound

Product 1

HCID 14134445HCID 14134445, compound

Procedure

By methods outlined in Example 2 and using methyl-2-isobutyl acrylate was made methyl-1-benzyloxycarbonylaminoethyl-[2-carbomethoxy-4-methyl-1-n-pentyl]phosphinate. NMR (D2O) 1.9 (overlapping d, 6H); 1.5-3.2 (m, 9H); 4.6 (d, 3H); 3.8-4.3 (m, 1H); 5.1 (s, 2H); 5.5 (d, 0.05H); 5.9 (d, 0.5H); 7.2 (s, 5H).

Sources & evidence

ORD record
ord-7f729321f572496f9c34dddc7d735a1f
Source dataset
uspto-grants-1987_12
Patent number
US04715994

Reaction notes

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