Dimethylamine → HCID 20156422, compound

HRID 986767Notes

Reaction equation

HRID 986767 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[C:6]([S:11](Cl)(=[O:13])=[O:12])=[CH:5][C:4]=1[C:15]1[N:16]=[C:17]2[N:22]=[CH:21][CH:20]=[CH:19][N:18]2[CH:23]=1.ClS(O)(=O)=O.[CH3:29][NH:30][CH3:31]>>[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[C:6]([S:11]([N:30]([CH3:31])[CH3:29])(=[O:13])=[O:12])=[CH:5][C:4]=1[C:15]1[N:16]=[C:17]2[N:22]=[CH:21][CH:20]=[CH:19][N:18]2[CH:23]=1

Participants

4

Reactant 3

HCID 674DimethylamineHCID 24638Chlorosulfonic acidHCID 20156424HCID 20156424, compound

Product 1

HCID 20156422HCID 20156422, compound

Procedure

Prepared from 2-(2,4-dimethoxy-5-chlorosulphonyl-phenyl)-imidazo[1,2-a]pyrimidine (prepared from 2-(2,4-dimethoxyphenyl[1,2-a]pyrimidine and chlorosulphonic acid) and 40% dimethylamine analogously to Example 25.

Sources & evidence

ORD record
ord-d33b90aa3c284a6e99c0df5f64082591
Source dataset
uspto-grants-1987_12
Patent number
US04716169

Reaction notes

Loading…