HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 86584589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | 2-Norbornene | HCID 10352 | — |
| Reactant | 5-Norbornene-2-carboxylic acid | HCID 78949 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86584589 | HCID 86584589 | 58% |
Reaction Steps
To 70 ml of tetrahydrofuran was added 0.05 M of norbornylene, 0.15 M of bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 0.2M of maleic anhydride and 0.4 g of AIBN. The resulting solution was reacted at 67° C. for 8 hours. Thereafter, a polymer was precipitated and filtered in petroleum ether/ether (1/1) solution, to obtain the title polymer (yield: 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630281B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-6a3d086cdaac46f4b4d796e285a05688 |
| Source note | uspto-grants-2003_10 |