HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 22987953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22987953 | HCID 22987953 | — |
Reaction Steps
207.0 g of 3,4-dimethoxybenzaldehyde, 100.0 g of ammonium acetate and 125 ml of nitromethane are heated to boiling for 34 h in 1.0 l of glacial acetic acid. After cooling in an ice bath, the precipitate is filtered off with suction, rinsed with glacial acetic acid and petroleum ether and dried. M.p.: 140-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630483B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-73c76a33b3fa4a0b9a244a0b447b9398 |
| Source note | uspto-grants-2003_10 |