1-(Bromomethyl)-4-chlorobenzene → HCID 22988178, compound
Reaction equation
[Cl:1][C:2]1[C:3]([CH2:12][N:13]2[C:22](=[O:23])[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[NH:15][C:14]2=[S:24])=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[Cl:25][C:26]1[CH:33]=[CH:32][C:29]([CH2:30]Br)=[CH:28][CH:27]=1>>[Cl:1][C:2]1[C:3]([CH2:12][N:13]2[C:22](=[O:23])[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[N:15]=[C:14]2[S:24][CH2:30][C:29]2[CH:32]=[CH:33][C:26]([Cl:25])=[CH:27][CH:28]=2)=[N:4][CH:5]=[C:6]([C:8]([F:9])([F:10])[F:11])[CH:7]=1Participants
3
Procedure
This compound was prepared from the product of Example 10 and 4-chlorobenzylbromide in analogous fashion to Example 8, m.p. 137° C.
Sources & evidence
- ORD record
- ord-91720da6f51d4785b14b0c13fe4a3d75
- Source dataset
- uspto-grants-2003_10
- Patent number
- US06630495B1
Reaction notes
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