Benzyl Chloride → HCID 22988138, compound

HRID 987070Notes

Reaction equation

HRID 987070 reaction equation
[NH:1]1[C:5]([C:6]([O:8][CH2:9][CH2:10]CC)=[O:7])=[CH:4][N:3]=[CH:2]1.[CH2:13](Cl)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH:13]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=[CH:15][C:14]=1[CH2:19][N:1]1[C:5]([C:6]([O:8][CH2:9][CH3:10])=[O:7])=[CH:4][N:3]=[CH:2]1

Participants

3

Reactant 2

HCID 7503Benzyl ChlorideHCID 22988126HCID 22988126, compound

Product 1

HCID 22988138HCID 22988138, compoundYield 162.3%

Procedure

2.4 g (17.1 mmol) of butyl imidazole-5-carboxylate were reacted with 4.1 g (32.1 mmol) of benzyl chloride analogously to procedure 8a. 7.3 g (78%) of the product were obtained.

Sources & evidence

ORD record
ord-e5199ee7f28a49f0a3e5bcc482a6a9ab
Source dataset
uspto-grants-2003_10
Patent number
US06630493B1

Reaction notes

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