HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 2-Ethoxy-3-{3-[3-(4-methylsulfonyloxyphenyl)propoxy]phenyl}propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Ethyl 2-ethoxy-3-{3-[3-(4-methylsulfonyloxyphenyl)propoxy]phenyl}propanoate | HCID 22988419 | — |
| Product | 2-Ethoxy-3-{3-[3-(4-methylsulfonyloxyphenyl)propoxy]phenyl}propanol | HCID 22988435 | 99% |
Reaction Steps
The compound was synthesised in an analogous method to Example 1 using ethyl 2-ethoxy-3-{3-[3-(4-methylsulfonyloxyphenyl)propoxy]phenyl}propanoate (0.642 g, 1.42 mmol) and sodium borohydride (93.26 mg, 2.47 mmol). The reaction was quenched after 28 hours to give 0.574 g (yield 99%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630509B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-85ddad4f97e44a0a95735f7385907e8f |
| Source note | uspto-grants-2003_10 |