HuagongsheHuagongshe Chemistry Print Report · For research reference only
Valeryl chloride → (4R,5S)-3-(1'-oxopentyl)-4-methyl-5-phenyl-2-oxazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Valeryl chloride | HCID 61186 | — |
| Reactant | (4R,5S)-(+)-4-Methyl-5-phenyl-2-oxazolidinone | HCID 2733812 | — |
| Reactant | (S)-4-benzyl-3-pentanoyloxazolidin-2-one | HCID 11391341 | — |
| Product | (4R,5S)-3-(1'-oxopentyl)-4-methyl-5-phenyl-2-oxazolidinone | HCID 12109355 | 84% |
Reaction Steps
(4R,5S)-3-(1′-oxopentyl)-4-methyl-5-phenyl-2-oxazolidinone was synthesized from (4R,5S)-4-methyl-5-phenyl-2-oxazolidinone and valeroyl chloride by the same procedure as (4S)-3-(1′-oxopentyl)-4-benzyl-2-oxazolidinone. The product (29.55 g) was obtained in 84% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630602B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-610e6e180d1e401a8268b090fbba3846 |
| Source note | uspto-grants-2003_10 |