HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Benzyloxyphenyl)-2-ethoxy-3-methylacrylic acid ethyl ester → HCID 54190417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Benzyloxyphenyl)-2-ethoxy-3-methylacrylic acid ethyl ester | HCID 54013513 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54190417 | HCID 54190417 | 94% |
Reaction Steps
3-(4-Benzyloxyphenyl)-2-ethoxy-3-methylacrylic acid ethyl ester (1.58 g; 4.64 mmole) was hydrogenated at atmospheric pressure in ethyl acetate (20 ml) using Pd/C (wet) as catalyst. After filtration through celite, the solvent was evaporated in vacuo to give (1.1 g; yield 94%) of 3-(4-hydroxyphenyl)-2-ethoxybutanoic acid ethyl ester as a diastereomeric mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630600B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-4d29bf98154a4b8bbfa5327c49dc6c1a |
| Source note | uspto-grants-2003_10 |