HCID 54470561, compound → HCID 22988726, compound

HRID 987321Notes

Reaction equation

HRID 987321 reaction equation
C([O:3][C:4](=[O:27])[CH:5]([O:24][CH2:25][CH3:26])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][C:16]2[CH:21]=[CH:20][C:19]([S:22][CH3:23])=[CH:18][CH:17]=2)=[CH:9][CH:8]=1)C>O1CCOCC1>[CH2:25]([O:24][CH:5]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][C:16]2[CH:17]=[CH:18][C:19]([S:22][CH3:23])=[CH:20][CH:21]=2)=[CH:9][CH:8]=1)[C:4]([OH:27])=[O:3])[CH3:26]

Participants

3

Reactant 1

HCID 54470561HCID 54470561, compound

Product 1

HCID 22988726HCID 22988726, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

2-Ethoxy-3-{4-[2-(4-methylsulfanylphenyl)ethoxy]phenyl}propanoic acid ethyl ester (described in Example 81) was hydrolyzed using the same method as in Example 2 but with dioxane instead of tetrahydrofuran to give 2-ethoxy-3-{4-[2-(4-methylsulfanylphenyl)ethoxy]-phenyl}propanoic acid.

Sources & evidence

ORD record
ord-c156303104e441319d8701e2d5034260
Source dataset
uspto-grants-2003_10
Patent number
US06630600B1

Reaction notes

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