1-Bromohexadecane → HCID 22987549, compound

HRID 987350Notes

Reaction equation

HRID 987350 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17].[OH:18][C:19]1[CH:20]=[C:21]([CH:24]=[C:25]([OH:27])[CH:26]=1)[CH:22]=[O:23]>>[CH2:2]([O:18][C:19]1[CH:20]=[C:21]([CH:24]=[C:25]([O:27][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH3:2])[CH:26]=1)[CH:22]=[O:23])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]

Participants

3

Reactant 2

HCID 82131-BromohexadecaneHCID 943653,5-Dihydroxybenzaldehyde

Product 1

HCID 22987549HCID 22987549, compound

Procedure

The title compound was prepared according to the method described in Example 9 above from 1-bromohexadecane and 3,5-dihydroxy-benzaldehyde. The solid reaction product was collected by filtration and washed with methyl ethyl ketone (Soxhlet). The filtrate was evaporated under reduced pressure to give the title compound as a red oil which was crystallised from acetone.

Workup

  1. customThe title compound was prepared
  2. customThe solid reaction product
  3. filtrationwas collected by filtration
  4. washwashed with methyl ethyl ketone (Soxhlet)
  5. customThe filtrate was evaporated under reduced pressure

Sources & evidence

ORD record
ord-512ba5a8cca94966b37c65d079b63807
Source dataset
uspto-grants-2003_10
Patent number
US06630128B1

Reaction notes

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