HCID 18008629, compound → HCID 136401072, compound

HRID 987367Notes

Reaction equation

HRID 987367 reaction equation
[CH:1]([C:4]1[CH:11]=[C:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:9]=[C:6]([CH:7]=O)[C:5]=1[OH:21])([CH3:3])[CH3:2].CC1C=C(CCCCCCCCC)C=C(C=[N:27][OH:28])C=1O>>[CH:1]([C:4]1[CH:11]=[C:10]([CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:9]=[C:6]([CH:7]=[N:27][OH:28])[C:5]=1[OH:21])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 18008629HCID 18008629, compoundHCID 136401071HCID 136401071, compound

Product 1

HCID 136401072HCID 136401072, compoundYield 96.1%

Procedure

Oximation and workup of 3-isopropyl-5-nonylsalicylaldehyde (3b) (57.6 g, 0.2 mol) as described for 1c gave 3-isopropyl-5-nonylsalicylaldoxime (58.21 g) in 96.1% yield.

Sources & evidence

ORD record
ord-03c82bf0ef7a4fe3b804a9ed4d0de94d
Source dataset
uspto-grants-2003_10
Patent number
US06632410B2

Reaction notes

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