HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Phosphate, Tribasic → 4-(Pyridin-3-yl)-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Phosphate, Tribasic | HCID 62657 | — |
| Reactant | 4-Bromo-2-nitroaniline | HCID 70132 | — |
| Reactant | 3-Pyridinylboronic acid | HCID 2734378 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(Pyridin-3-yl)-2-nitroaniline | HCID 10465859 | — |
Reaction Steps
To a solution of 4-bromo-2-nitroaniline (217 mg, 1 mmol) in DMF (6 mL) was added 3-pyridine boronic acid (148 mg, 1.2 mmol), potassium phosphate (276 mg, 1.3 mmol), and dichloro-(diphenylphosphinoferrocene)palladium (75 mg, 0.1 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632809B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-0169070dacc84ca9977222d833841453 |
| Source note | uspto-grants-2003_10 |