HCID 22476268, compound → 4,7-Dimethoxy-1H-pyrrolo[2,3-c]pyridine

HRID 987544Notes

Reaction equation

HRID 987544 reaction equation
C(N1CCN(C(=O)C([C:18]2[C:26]3[C:21](=[C:22]([O:29][CH3:30])[N:23]=[CH:24][C:25]=3[O:27][CH3:28])[NH:20][CH:19]=2)=O)C(C)C1)(=O)C1C=CC=CC=1.COC1C=NC(OC)=C2C=1C(C(=O)C([O-])=O)=CN2.[K+]>>[CH3:28][O:27][C:25]1[CH:24]=[N:23][C:22]([O:29][CH3:30])=[C:21]2[C:26]=1[CH:18]=[CH:19][NH:20]2

Participants

3

Reactant 2

HCID 22476268HCID 22476268, compoundHCID 22893810Potassium (4,7-dimethoxy-6-azaindol-3-yl)-oxoacetate

Product 1

HCID 224762954,7-Dimethoxy-1H-pyrrolo[2,3-c]pyridine

Procedure

Compound 5ap, {circle around (R)}N-(benzoyl)-3-methyl-N′-[(4,7-dimethoxy-6-azaindol-3-yl)-oxoacetyl]piperazine (white solid) was prepared using the same method used to prepare compound 5a except that Potassium (4,7-dimethoxy-6-azaindol-3-yl)-oxoacetate was used as the starting material. MS m/z: (M+H)+ calcd for C23H25N4O5: 437.18; found 437.24. HPLC retention time: 1.37 minutes (column B).

Sources & evidence

ORD record
ord-7ce9117157144bd7b0b8a0126c95a21e
Source dataset
uspto-grants-2003_10
Patent number
US06632819B1

Reaction notes

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