HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 18009475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 68834656 | HCID 68834656 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18009475 | HCID 18009475 | — |
Reaction Steps
A mixture of 1-carboxymethylidenyl-4-phenyl-4-(3-(2-methoxyphenyl)-3-oxo-2-azaprop-1-yl)-cyclohexane (Example 174, 64 mg, 0.17 mmol) and Pd/C (10 mg, 10%), in 5.0 mL of EtOAc was shaken under 50 psi of hydrogen for 24 h. The mixture was filtered through a plug of silica gel and concentrated to give the title compound as a mixture of isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632836B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-d4d15155aadf40408685c383ee36f3e0 |
| Source note | uspto-grants-2003_10 |