HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylacetic acid → N-(Cyclopentylacetyl)-L-alanine Methyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylacetic acid | HCID 71606 | — |
| Reactant | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| Product | N-(Cyclopentylacetyl)-L-alanine Methyl Ester | HCID 54564390 | — |
Reaction Steps
Following General Procedure A above using cyclopentylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as a solid having a melting point of 43-46° C. Purification was by recrystallization from ethyl acetate/hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632811B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-9caeda3d7f0d4760b2cf4400e3e67a80 |
| Source note | uspto-grants-2003_10 |