HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11558572, compound → HCID 10165414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11558572 | HCID 11558572 | — |
| Reactant | (2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid | HCID 12135350 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10165414 | HCID 10165414 | — |
Reaction Steps
Following General Procedure D and using N-(3,5-difluorophenylacetyl)-L-alanine (Ex. B) and 5-amino-7-(2′,2′,2′-trifluoroethyl)-5,7-dihydro-6H-dibenz[b d]azepin-6-one (Example 7-M), the title compound was prepared. The reaction was monitored by tlc (Rf=0.15, 5% MeOH/CHCl3) and product was purified by chromatography (silica, 5% MeOH/CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632811B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-da4d8a0959d04eb3b66348e79392090e |
| Source note | uspto-grants-2003_10 |