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HRID 987756作成日：2026年10月25日

4-Chloroaniline → N-(4-chlorophenyl)alanine Iso-butyl Ester

https://huagongshe.com/reaction/987756

反応式

関与物質

役割名称HCID仕込み量
反応物4-ChloroanilineHCID 7812—
反応物Isobutyl pyruvateHCID 83084—
生成物N-(4-chlorophenyl)alanine Iso-butyl EsterHCID 54074575—

反応手順

Following General Procedure AA above and using 4-chloroaniline (Aldrich) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.6 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06632811B2
出典データセットuspto-grants-2003_10
ORD IDord-99ce215b52ef4a0d8f8514cd32f5f046
出典メモuspto-grants-2003_10