HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthylamine → N-(2-naphthyl)alanine isobutyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthylamine | HCID 7057 | — |
| Reactant | Isobutyl pyruvate | HCID 83084 | — |
| Product | N-(2-naphthyl)alanine isobutyl ester | HCID 54457376 | — |
Reaction Steps
Following General Procedure AA above and using 2-aminonaphthalene (Aldrich) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. Purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632811B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-d1ea2d5fc99f41c3af36f25af395c912 |
| Source note | uspto-grants-2003_10 |