HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11123605, compound → HCID 15291043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11123605 | HCID 11123605 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15291043 | HCID 15291043 | 104.4% |
Reaction Steps
29.3 g (61.6 mmol) of Z-Val-MeVal-Pro-OMe were dissolved in 230 ml of methanol. After addition of 1.15 g of 10% palladium/charcoal, the reaction mixture was hydrogenated. Filtration and evaporation to dryness yielded 21.96 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632795B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-b984ad4eb2ad48978761a215e4bc96e6 |
| Source note | uspto-grants-2003_10 |