HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22345427, compound → HCID 69793583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22345427 | HCID 22345427 | — |
| Reactant | Ethyl 3-[3-(3-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)-4-methoxyphenyl)acrylate | HCID 69792380 | — |
| Product | HCID 69793583 | HCID 69793583 | 89.3% |
Reaction Steps
In a manner similar to that of Example 1(a), by reaction of 2.5 g (6.12 mmol) of ethyl 3-[3-(3-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)-4-methoxyphenyl]acrylate obtained in Example 13(f) with 1.26 g (6.73 mmol) of 3-methoxymethoxybenzyl chloride obtained above, 2.90 g (85%) of the expected compound were obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632963B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-5ef852eeed3046b48fe9bed0135abae8 |
| Source note | uspto-grants-2003_10 |