HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69792697, compound → HCID 69792524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69792697 | HCID 69792697 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69792524 | HCID 69792524 | 83.4% |
Reaction Steps
In a manner similar to that of Example 2(g) but in ethanol as solvent, starting from 1.9 g (3.4 mmol) of ethyl 3-{4-methoxy-3-[3-(3-methoxymethoxybenzyloxy)-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl]phenyl}acrylate obtained in Example 30(d), 1.38 g (79%) of the expected compound was obtained in the form of a white powder having a melting point of 131°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632963B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-f9625e1f27144d1ea973e7dbf4d72058 |
| Source note | uspto-grants-2003_10 |