Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 69132345 | HCID 69132345 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69132794 | HCID 69132794 | 10.3% |
Reaction Steps
A reaction mixture containing compound B (0.05 g, 0.16 mmole; obtained from Example 14), benzoyl chloride (15 ml, 0.16 mmole) and 50 mL of chloroform was heated to 150° C. for 2 hr. Chloroform was removed in vacuo to produce a residue. The residue was chromatographied using silica gel column with a developing solvent (CH2Cl2) to give 0.007 g (10%) of Compound 15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06635649B2 |
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| Source dataset | uspto-grants-2003_10 |
|---|
| ORD ID | ord-9f48011a9e4243f0bd35e3f2885f24d2 |
|---|
| Source note | uspto-grants-2003_10 |
|---|
