HCID 178474252, compound → HCID 178478631, compound

HRID 988915Notes

Reaction equation

HRID 988915 reaction equation
[Cl-:1].C([NH:5][C:6]1[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][C:7]=1[O:8][CH2:9][CH2:10][CH2:11][N+:12]1[CH:16]=[CH:15][N:14]([CH3:17])[CH:13]=1)(=O)C>C(O)C>[Cl-:1].[ClH:1].[ClH:1].[NH2:5][C:6]1[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][C:7]=1[O:8][CH2:9][CH2:10][CH2:11][N+:12]1[CH:16]=[CH:15][N:14]([CH3:17])[CH:13]=1

Participants

3

Reactant 1

HCID 178474252HCID 178474252, compound

Product 1

HCID 178478631HCID 178478631, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The 1-[3-(2-acetylamino-5-aminophenoxy)propyl]-3-methyl-3H-imidazol-1-ium chloride obtained in the above step (19.0 g) was dissolved, at room temperature and with stirring, in 90 ml of approximately 5N absolute hydrochloric ethanol.

Workup

  1. dissolutionwas dissolved, at room temperature

Sources & evidence

ORD record
ord-bb36b5b293d24d168ef7c25584f8ca01
Source dataset
uspto-grants-2003_10
Patent number
US06638321B1

Reaction notes

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