HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-1-propanamine → HCID 4780362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | 2-Chloro-5-nitrobenzonitrile | HCID 85504 | — |
| Product | HCID 4780362 | HCID 4780362 | 52% |
Reaction Steps
Starting with 36.5 g (0.2 mol) of 2-chloro-5-nitrobenzonitrile and 31.3 g (0.25 mol) of 3-imidazol-1-ylpropylamine, and after purification by recrystallization from refluxing at 96 ° ethanol, 28.2 g of yellow crystals melting at 177° C. (Kofler) were obtained, the elemental analysis of which, calculated for C13H13N5O2, was:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638321B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-07f11ec90a42433db1e57ec8a27caaf9 |
| Source note | uspto-grants-2003_10 |