1-Methylimidazole → HCID 178493301, compound

HRID 988921Notes

Reaction equation

HRID 988921 reaction equation
[Br:1][CH2:2][CH2:3][NH:4][C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][C:6]=1[O:14][CH3:15].[CH3:16][N:17]1[CH:21]=[CH:20][N:19]=[CH:18]1>C1(C)C=CC=CC=1>[Br-:1].[CH3:15][O:14][C:6]1[CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[CH:9]=[CH:10][C:5]=1[NH:4][CH2:3][CH2:2][N+:19]1[CH:20]=[CH:21][N:17]([CH3:16])[CH:18]=1

Participants

4

Reactant 2

HCID 13901-MethylimidazoleHCID 18003895HCID 18003895, compound

Product 1

HCID 178493301HCID 178493301, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A mixture of 46.8 g (0.17 mol) of (2-bromoethyl)-(2-methoxy-4-nitrophenyl)amine and 20.5 g (0.25 mol) of 1-methyl-1H-imidazole in 170 ml of toluene was refluxed for 7 hours.

Workup

  1. temperaturewas refluxed for 7 hours

Sources & evidence

ORD record
ord-03e9f15a9a584b28b6a898f4b0da3f27
Source dataset
uspto-grants-2003_10
Patent number
US06638321B1

Reaction notes

Loading…