1,4-bis(chloromethyl)-2-(3,7-dimethyloctyloxy)-5-methoxybenzene → HCID 68619000, compound

Participants

Reaction Steps

7.47 g (28.5 mmol) of 1,4-bis(chloromethyl)-2-(3,7-dimethyloctyloxy)-5-methoxybenzene (Ex. Z1), 6.22 g (17.1 mmol) of 2,5-bis(chloromethyl)4-methoxy-3′-(3,7-dimethyloctyloxy)biphenyl (Ex. E2) and 4.64 g (11.4 mmol) of 2,5-bis(chloromethyl-3′-(3,7-dimethyloctyloxy)biphenyl (Ex. Z3) in 3450 ml of dry 1,4-dioxane were polymerized at 98-100° C. analogously to

Provenance & Evidence