HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Alanine → p-Toluenesulfonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Alanine | HCID 5950 | — |
| Reactant | Cyclohexanol | HCID 7966 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | p-Toluenesulfonic acid | HCID 6101 | — |
Reaction Steps
This was synthesised according to Standard Procedure 2, using L-Alanine (2.0 g, 22.5 mmol), cyclohexanol (2.34 ml, 22.5 mmol), p-toluene sulfonic acid monohydrate (4.7 g, 24.7 mmol), and toluene (100 ml). The p-toluene sulfonate salt was isolated as a pale orange solid (1.45 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638919B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-bcbc99c232284a1caa59a3933534ddee |
| Source note | uspto-grants-2003_10 |