HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → (6-Isocyano-hexyl)-(2-pyridin-2-yl-imidazo[1,2-a]pyridin-3-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Reactant | 1,6-Diisocyanohexane | HCID 3391105 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | (6-Isocyano-hexyl)-(2-pyridin-2-yl-imidazo[1,2-a]pyridin-3-yl)-amine | HCID 9927052 | — |
Reaction Steps
Compound (1) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml 1,6-diisocyanohexane solution (0.2 M, MC), 0.500 ml pyridine-2-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-048f5a4606cd44e6a14ed5e3aacc30f6 |
| Source note | uspto-grants-2003_10 |