HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-vinyl-2-pyrrolidone → 1-Phenyl-1H-1,2,3-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | Azidobenzene | HCID 69319 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Phenyl-1H-1,2,3-triazole | HCID 270009 | — |
Reaction Steps
In the method of preparation, the reaction between the N-vinylpyrrolidinone and the phenyl azide is carried out at room temperature in ethanol as solvent, and allowed to stand in the dark for several weeks, depending on the reactivity of the phenyl azides. Refluxing the reaction mixture eliminates the 5-(2-oxo-1-pyrrolidino) group and yields the 1-phenyl triazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638954B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-2822d6e2988e481b8fd1cca2403860b8 |
| Source note | uspto-grants-2003_10 |