HuagongsheHuagongshe Chemistry Print Report · For research reference only
MLS000756500 → 3-Amino-N-pyridin-3-ylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | MLS000756500 | HCID 308753 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Amino-N-pyridin-3-ylbenzamide | HCID 12109483 | 86% |
Reaction Steps
A solution of 3-(3-nitrobenzoylamino)-pyridine (2 g, 8.23 mmol) in ethanol (200 ml) was treated with 10% palladium on charcoal (0.5 g) and hydrogenated at atmospheric pressure for 4 h. Filtration and evaporation afforded the product as a white solid (1.51 g, 86%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638953B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-5612c0241b86421b83bede928603f868 |
| Source note | uspto-grants-2003_10 |