HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-6-(trifluoromethyl)indoline → HCID 10670813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-6-(trifluoromethyl)indoline | HCID 11206713 | — |
| Reactant | HCID 18005169 | HCID 18005169 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10670813 | HCID 10670813 | 41.9% |
Reaction Steps
The title compound (0.15 g, 40%) was prepared as a tan powder using the methodology of Example 28 from phenyl N-(3-ethyl-5-(pyrid-3-yl)phenyl carbamate (D30) (0.26 g, 0.81 mmol) and 5-methoxy-6-trifluoromethyl indoline (D11) (0.177 g, 0.81 mmol) in DMF (10 ml). Melting point: 205° C.-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638953B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-1cd8815db3ee472bb11a7bd3b8911faa |
| Source note | uspto-grants-2003_10 |