Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → HCID 18005526, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | tert-Butyl(dimethyl){[3-(2-methylbenzylidene)-1-cyclohepten-1-yl]oxy}silane | HCID 69965728 | — |
| 생성물 | HCID 18005526 | HCID 18005526 | — |
반응 단계
A solution of n-tetra-n-butylammonium fluoride (1M) in THF (1.35 mmol) is added using a syringe to a solution of the compound obtained in Step A (1.34 mmol) in 15 ml of anhydrous THF at 0° C., and the whole is stirred at that temperature for 1 hour 30 minutes. The reaction mixture is then concentrated to dryness and deposited directly over a column of silica gel (heptane/AcOEt 9/1) to yield the title product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06638962B2 |
| 출처 데이터셋 | uspto-grants-2003_10 |
| ORD ID | ord-8ab77105869e4e05b0462a40eb1a982f |
| 출처 메모 | uspto-grants-2003_10 |