HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Dicyclopentadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Cyclopentadiene | HCID 7612 | — |
| Reactant | Acrylate | HCID 25188 | — |
| Product | Dicyclopentadiene | HCID 6492 | — |
Reaction Steps
The derivative was synthesized as follows. 20 grams of the derivative of acrylate obtained as the third example was dissolved in 20 milliliters of toluene. 7 grams of cyclopentadiene was dropped into the solution cooled with ice, and was agitated through all night. Dicyclopentadiene was produced as byproduct, and was eliminated in vacuum. Then, 24.9 grams of the derivative of norbornene was obtained. The derivative of norbornene was viscous liquid, and the yield was 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06639084B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-c6e9df7905114349b2087f3b9bfa59c0 |
| Source note | uspto-grants-2003_10 |