N-Acetyl-L-Cysteine → HCID 86583714, compound
Reaction equation
[Cl-].[Cr+3:2].[Cl-].[Cl-].[C:5]([NH:8][C@H:9]([C:12]([OH:14])=[O:13])[CH2:10][SH:11])(=[O:7])[CH3:6]>O>[C:5]([NH:8][C@H:9]([C:12]([OH:14])=[O:13])[CH2:10][SH:11])(=[O:7])[CH3:6].[Cr:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 40 °C
Procedure
One half gram (1.85 mmole) of chromium chloride (CrCl3) was dissolved in 30 ml of deionized water to get a green solution. 1.5 g (9.2 mmole) of N-acetyl cysteine (NAC) was dissolved in 40 ml of deionized water were added, and the mixture was stirred for 3 hours at 40° C. until the solution turned dark green-blue.
Workup
- customto get a green solution
- additionwere added
Sources & evidence
- ORD record
- ord-0c3ac33c41a745a1b76c3f1c3d78483d
- Source dataset
- uspto-grants-2002_10
- Patent number
- US06458351B2
Reaction notes
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