N-bromobutanimide → HCID 131723532, compound

Participants

Reaction Steps

To a stirred solution of the compound (200 mg) of Example 16 in methanol and water (7.5 mL/0.5 mL), was added N-bromosuccinimide (73 mg). The mixture was allowed to stir for 1 h, and solvent was removed. The residue was purified by silica gel column chromatography (ethyl acetate/hexanes) to give a solid (90 mg, 35%). (M+H): 564.

Provenance & Evidence