Chlorosulfamic acid → HCID 70157361, compound

HRID 989691Notes

Reaction equation

Cl.[C:2]([C:4]1[CH:5]=[CH:6][C:7]2[N:13](CC3C=NC=CC=3)[CH2:12][C@@H:11]([CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[N:10]([S:28](C3SC=CC=3)(=[O:30])=[O:29])[CH2:9][C:8]=2[CH:36]=1)#[N:3].S(Cl)(=O)(=O)[NH2:38]>>[C:2]([C:4]1[CH:5]=[CH:6][C:7]2[NH:13][CH2:12][C@@H:11]([CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[N:10]([S:28]([NH2:38])(=[O:30])=[O:29])[CH2:9][C:8]=2[CH:36]=1)#[N:3]

Participants

Reactant 2

HCID 24499Chlorosulfamic acid

HCID 131723534HCID 131723534, compound

Product 1

HCID 70157361HCID 70157361, compound

Procedure

The title compound was prepared from Compound A of Example 23 and sulfamyl chloride following the procedure of Compound B of Example 37.

Sources & evidence

ORD record: ord-09a466f7e2b94498a6d0d8a8217addc9
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06458783B1

Reaction notes

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