HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 22313246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | HCID 21813589 | HCID 21813589 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22313246 | HCID 22313246 | 55% |
Reaction Steps
A mixture of 3-(2-amino-4-chloro-6-methylpyrimidine-5-yl)propanenitrile (500 mg, 2.54 mmol), amylamine (2.94 ml) and dioxane (5 ml) was kept at 90° C. for 8.5 hours. The procedure according to pro-treatment of Example 23 was carried out to give the object compound (346 mg, 55.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458798B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-c74bac2f2ee84754be240a798a16cb7a |
| Source note | uspto-grants-2002_10 |