反应详情

温度

50 °C

15.0 g (67.46 mmol) of 1-ethyl-heptyl methanesulphonate are dissolved in 300 ml of DMSO and, after addition of 17.54 g (269.8 mmol) of sodium azide, the mixture is stirred at 50° C. for 16 hours. The reaction mixture is poured into ice-water and extracted three times with ether. The extract is dried over sodium sulphate giving 11.4 g (96%) of a yellow liquid.

1. extractionextracted three times with ether
2. dry with materialThe extract is dried over sodium sulphate giving 11.4 g (96%) of a yellow liquid