Methyl 4-pyridylacetate → HCID 135484595, compound

HRID 989733Notes

Reaction equation

HRID 989733 reaction equation
[NH2:1][C:2]1[N:6]([CH:7]([CH3:17])[CH2:8][CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[N:5]=[N:4][C:3]=1[C:18]([NH2:20])=[O:19].[N:21]1[CH:26]=[CH:25][C:24]([CH2:27][C:28](OC)=O)=[CH:23][CH:22]=1>>[CH3:17][CH:7]([N:6]1[C:2]2[N:1]=[C:28]([CH2:27][C:24]3[CH:25]=[CH:26][N:21]=[CH:22][CH:23]=3)[NH:20][C:18](=[O:19])[C:3]=2[N:4]=[N:5]1)[CH2:8][CH2:9][CH2:10][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1

Participants

3

Procedure

Analogously to the procedure of Example 1, the title compound is prepared from 1.0 g (3.8 mmol) of 5-amino-1-(1-methyl-4-phenyl-butyl)-1H-[1,2,3]triazole-4-carboxamide and 2.21 g (14.6 mmol) of methyl 4-pyridylacetate.

Sources & evidence

ORD record
ord-e3034574619e4d44b50b3b7dd9e0af7a
Source dataset
uspto-grants-2002_10
Patent number
US06458796B1

Reaction notes

Loading…