HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Diisopropyl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 69948620 | HCID 69948620 | — |
| Product | Diisopropyl Ether | HCID 7914 | — |
| Product | HCID 70027424 | HCID 70027424 | — |
Reaction Steps
3 ml of 2N hydrochloric acid is added to 339 mg of the ethyl ester of Example 3 in 20 ml of THF, the reaction medium is agitated for 10 minutes and evaporated under reduced pressure while adding toluene. After treatment with ether and isopropyl ether, 312 mg of the expected hydrochloric acid salt is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458801B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-4880a3b056f94853a7eb58ec04c3c9f3 |
| Source note | uspto-grants-2002_10 |