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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 989928Generated: October 30, 2026

Trifluoroacetic acid → HCID 23387352, compound

https://huagongshe.com/reaction/989928

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 23387543HCID 23387543—
SolventDichloromethaneHCID 6344—
ProductHCID 23387352HCID 23387352—

Reaction Steps

To a solution of 4-methoxybenzyl 2-(N-CBZ-L-valyloxy)-propionate (7.8 g, 17.5 mmole) in dichloromethane (100 ml) was added trifluoroacetic acid (10 ml) and the solution was stirred for one hour at room temperature. The solution was evaporated under reduced pressure and the product was isolated by silica gel column chromatography. Yield: 5.0 g

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06458772B1
Source datasetuspto-grants-2002_10
ORD IDord-290c2686816e4d0e81846bf49d8cfd96
Source noteuspto-grants-2002_10