HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54108173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 54221625 | HCID 54221625 | — |
| Product | HCID 54108173 | HCID 54108173 | — |
Reaction Steps
2-(N-benzyloxycarbonyl-L-valyloxy)-3-methyl-(S)-(+)-butyric acid was esterified by the method described in Example A-I-1, step d. The title compound (2.96 g) was obtained after silica gel column chromatography (0, 1, 2% ethanol in dichloromethane). Rf (2%MeOH/CHCl3) 0.85.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458772B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-40962a870d3a4b7797bd854c82f2c418 |
| Source note | uspto-grants-2002_10 |