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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 989997Generated: October 29, 2026

HCID 23387560, compound → HCID 23387533, compound

https://huagongshe.com/reaction/989997

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23387560HCID 23387560—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 23387533HCID 23387533—

Reaction Steps

A solution of benzyl 3-(N-FMOC-L-valyloxy )-2-stearoyloxypropionate (0.78 g, 1 mmole) in 20 ml ethyl acetate was hydrogenated with 10% palladium on charcoal (0.2 g) at normal pressure for three hours at room temperature. The catalyst was filtered and washed with ethyl acetate and 1,4-dioxane. The solution was evaporated under reduced pressure. Yield: 0.63 g=90%

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06458772B1
Source datasetuspto-grants-2002_10
ORD IDord-adc4b3826413407d8877ac755b7e8741
Source noteuspto-grants-2002_10