HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23387560, compound → HCID 23387533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23387560 | HCID 23387560 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23387533 | HCID 23387533 | — |
Reaction Steps
A solution of benzyl 3-(N-FMOC-L-valyloxy )-2-stearoyloxypropionate (0.78 g, 1 mmole) in 20 ml ethyl acetate was hydrogenated with 10% palladium on charcoal (0.2 g) at normal pressure for three hours at room temperature. The catalyst was filtered and washed with ethyl acetate and 1,4-dioxane. The solution was evaporated under reduced pressure. Yield: 0.63 g=90%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458772B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-adc4b3826413407d8877ac755b7e8741 |
| Source note | uspto-grants-2002_10 |