HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17927434, compound → HCID 18406004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17927434 | HCID 17927434 | — |
| Reactant | HCID 22954338 | HCID 22954338 | — |
| Product | HCID 18406004 | HCID 18406004 | 16% |
Reaction Steps
Using the general procedure described in example 41, starting with 1-(3-bromopropyl)cyclobutanecarboxylic acid ethyl ester, 1-[3-(methylthio)propyl]cyclobutanecarboxylic acid ethyl ester was prepared in 58% yield as a colorless oil. HR MS: Obs. mass, 216.1182. Calcd. mass, 216.1184 (M+). Also, 1-[3-(methylthio)propyl]cyclobutanecarboxylic acid was obtained in 16% yield as a colorless oil. HR MS: Obs. mass, 188.0872. Calcd. mass, 188.0871 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458844B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-d9e0d4f8bb5f4a81bdaff1e00bf6c5c5 |
| Source note | uspto-grants-2002_10 |