1-Butanol → Butyl Acrylate

HRID 990300Notes

Reaction equation

HRID 990300 reaction equation
O.[CH2:2]([OH:6])[CH2:3][CH2:4][CH3:5].C([O:10][CH2:11][CH2:12][CH2:13]C)(=O)C>>[C:11]([O:6][CH2:2][CH2:3][CH2:4][CH3:5])(=[O:10])[CH:12]=[CH2:13]

Participants

4

Reactant 3

HCID 2631-ButanolHCID 962WaterHCID 31272Butyl Acetate

Product 1

HCID 8846Butyl Acrylate

Procedure

At the top of the column, a mixture of water, butanol, butyl acetate and butyl acrylate was obtained which separated into an aqueous phase and an organic phase; after the addition of 300 ppm of phenothiazine, the organic phase was supplied as reflux to the column.

Sources & evidence

ORD record
ord-3ea47f6590e64478b32c25ef21e9048f
Source dataset
uspto-grants-2002_10
Patent number
US06458989B1

Reaction notes

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