HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 2-fluoro-1,3-dimethylimidazolinium Iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Iodide Ion | HCID 30165 | — |
| Reactant | 2-Fluoro-1,3-dimethylimidazolidine | HCID 17871734 | — |
| Reactant | 2-Fluoro-1,3-dimethylimidazolinium | HCID 53443344 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-fluoro-1,3-dimethylimidazolinium Iodide | HCID 53443211 | — |
Reaction Steps
To a 300 ml four necked flask, 13.56 g (0.10 mol) of 2-fluoro-1,3-dimethylimidazolidine (DFI), 15.0 g (0.10 mol) of sodium iodide and 125 g of acetonitrile were charged and reacted at 250° C. for 4 hours in a nitrogen atmosphere under light shielding. The yield of 2-fluoro-1,3-dimethylimidazolinium=iodide (DMFI) was 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458990B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-82d5c8a2a9d2480a9ea1ee4ea25dc3f5 |
| Source note | uspto-grants-2002_10 |