Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 178478630, compound

HRID 990573Notes

Reaction equation

HRID 990573 reaction equation
[Cl-:1].[NH2:2][C:3]1[CH:18]=[C:17]([NH2:19])[CH:16]=[CH:15][C:4]=1[O:5][CH2:6][CH2:7][CH2:8][N+:9]1[CH:13]=[CH:12][N:11]([CH3:14])[CH:10]=1.C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl>>[ClH:1].[ClH:1].[Cl-:1].[NH2:2][C:3]1[CH:18]=[C:17]([NH2:19])[CH:16]=[CH:15][C:4]=1[O:5][CH2:6][CH2:7][CH2:8][N+:9]1[CH:13]=[CH:12][N:11]([CH3:14])[CH:10]=1

Participants

3

Reactant 2

HCID 149026Tetrafluoro-m-phenylenediamine dihydrochlorideHCID 178480881HCID 178480881, compound

Product 1

HCID 178478630HCID 178478630, compound

Procedure

12.7 g of white crystals of 1-[3-(2,4-diaminophenoxy)propyl]-3-methyl-3H-imidazol-1-ium chloride, dihydrochloride were obtained, melting with decomposition at above 260° C. (Kofler), and the elemental analysis of which, calculated for C13H21N4OCl3 was:

Sources & evidence

ORD record
ord-95a9af20166d408a9de81b152b5d94fc
Source dataset
uspto-grants-2002_10
Patent number
US06461389B1

Reaction notes

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