反应详情

4-Fluoronitrobenzene (5 g) and morpholine (7.2 g) were dissolved in ethanol (50 ml) and refluxed for 2 hr, before the ethanol was removed in vacuo. The resulting slurry was dissolved in ethyl acetate (30 ml) and washed with water (20 ml), dried over magnesium sulphate (2 g), and the solvent removed in vacuo to yield the title compound as an orange solid (7.3 g).

1. customwas removed in vacuo
2. dissolutionThe resulting slurry was dissolved in ethyl acetate (30 ml)
3. washwashed with water (20 ml)
4. dry with materialdried over magnesium sulphate (2 g)
5. customthe solvent removed in vacuo