HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53677822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Fluorobenzoyl chloride | HCID 9808 | — |
| Reactant | tert-Butyl (4-aminophenyl)carbamate | HCID 688611 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53677822 | HCID 53677822 | — |
Reaction Steps
To a solution of mono-N-(t-butoxycarbonyl)-1,4-phenylenediamine (1.58 g) and triethylamine (1.50 mL) in 25 mL of dichloromethane is added o-fluorobenzoyl chloride (1.20 g). A solid formed immediately forms and is filtered and washed with fresh solvent to yield a white solid, 1.90 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462055B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-6c48b3da29ce48f890fa62e8a0b0520a |
| Source note | uspto-grants-2002_10 |